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NMR of small organics


EMSL Project ID
3428

Abstract

We are synthesizing small organic crosslinkers and dye derivatives. We would like to analyze their composition and purity by 1D proton (and potentially carbon) NMR in deuterated solvents. In most cases we have large enough quantities that no more than a 15 minute acquisition should be required. We expect to have about ten samples/month, though there will be months when we will not be doing synthesis.

Project Details

Project type
Capability Research
Start Date
2003-03-23
End Date
2004-03-31
Status
Closed

Team

Principal Investigator

M. Mayer-Cumblidge
Institution
Pacific Northwest National Laboratory

Team Members

Thomas Squier
Institution
Western University of Health Sciences

Related Publications

Chen B, MUljana Mayer, and TC Squier. 2005. "Structural Uncoupling between Opposing Domains of Oxidized Calmodulin Underlies the Enhanced Binding Affinity and Inhibition of the Plasma Membrane Ca-ATPase." Biochemistry 44(12):4737-4747.
Mayer MUljana, L Shi, and TC Squier. 2005. "One-step, non-denaturing isolation of an RNA polymerase enzyme complex using an improved multi-use affinity probe resin." Molecular Biosystems 1(1):53-56.