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Site-Specific Sample Preparation of Surfaces and Buried Interfaces
for TEM and Atom Probe Analysis


EMSL Project ID
35190

Abstract

Technique development of methods for preparing cross-sectional TEM samples and atom-probe needle samples with the new dual-beam FIB instrument is proposed. Prior experience in FIB sample preparation with earlier-generation instruments offsite has demonstrate the need to develop sophisticated methods and strong user proficiency to effectively use the FIB. The work would involve several scientist /engineers at PNNL as well as Bruce Arey from the EMSL. The work is expected to yield suitable specimens from environmentally degraded alloys, and to lead to more demanding applications including 3-dimensional reconstruction of defective materials from FIB-cut samples.

Project Details

Project type
Large-Scale EMSL Research
Start Date
2009-10-06
End Date
2011-09-30
Status
Closed

Team

Principal Investigator

Matthew Olszta
Institution
Pacific Northwest National Laboratory

Team Members

David Catalini
Institution
Pacific Northwest National Laboratory

Daniel Schreiber
Institution
Pacific Northwest National Laboratory

Larry Thomas
Institution
Pacific Northwest National Laboratory

Bruce Arey
Institution
Pacific Northwest National Laboratory

Related Publications

Olszta MJ, DK Schreiber, LE Thomas, and SM Bruemmer. 2011. "Electron Microscopy Characterizations and Atom Probe Tomography of Intergranular Attack in Alloy 600 Exposed to PWR Primary Water." In 15th Environmental Degradation of Nuclear Materials . PNNL-SA-81560, Pacific Northwest National Laboratory, Richland, WA.
Olszta MJ, DK Schreiber, LE Thomas, and SM Bruemmer. 2011. "Electron Microscopy Characterizations and Atom Probe Tomography of Intergranular Attack in Alloy 600 Exposed to PWR Primary Water." In 15th Environmental Degradation of Nuclear Materials . PNNL-SA-81560, Pacific Northwest National Laboratory, Richland, WA.
Olszta MJ, DK Schreiber, LE Thomas, and SM Bruemmer. 2011. "Penetrative Internal Oxidation from Alloy 690 Surfaces and Stress Corrosion Crack Walls during Exposure to PWR Primary Water." In 15th Environmental Degradation of Nuclear Materials. PNNL-SA-81561, Pacific Northwest National Laboratory, Richland, WA.